Oxalate (C2O42-)

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AIM: – To identify the given inorganic compound for its acidic and basic radical.

APPARATUS:- Chemical Reagent, Test Tube, Test Tube holder, Spatula

PROCEDURE:-

Preliminary Test:-

Experiment Observation Inference
Added dilute sulphuric acid to given salt. No effect. Carbonate, sulphide , sulphite, nitrate absent.
Added concentrated sulphuric acid to given salt. Colourless gas with brisk effervescence evolved. Oxalate may be present.

Confirmatory Test:-

Experiment Observation Inference
Passed the above evolved gas through lime water . Lime water turned milky. Oxalate confirmed.

Chemical Equations:-

C2O42-  + H2SO4(aq) ==> CO(g) + CO2(g) + H2O(l) + SO42-

CO2(g) + Ca(OH)2(aq) ==>CaCO3(s)(milky) + H2O(l)

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